Magnetic Dual-template Molecularly Imprinted Polymer Nanoparticles for the Simultaneous Determination of Acetaminophen and Codeine in Urine Samples by Ion Mobility Spectrometry

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Magnetic Dual-template Molecularly Imprinted Polymer Nanoparticles for the Simultaneous Determination of Acetaminophen and Codeine in Urine Samples by Ion Mobility Spectrometry.

Dual-template magnetic molecularly imprinted polymer nanoparticles were synthesized and used for the solid-phase extraction of acetaminophen and codeine before simultaneous determination by corona discharge ion mobility spectrometry. The magnetic molecularly imprinted polymer nanoparticles were prepared using silica-coated magnetic nanoparticles as supporters, acetaminophen and codeine as templ...

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Application of Ion Mobility Spectrometry for Determination of Morphine in Human Urine

In this study, a rapid, simple and sensitive ion mobility spectrometry (IMS) method with corona discharge as ionization source was described for the morphine determination in human urine. Morphine was extracted and purified from urine samples using solid phase extraction procedure with C18 column. It can offer the clean extracts which no extra peaks were observed in IMS. Under operating experim...

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SYNTHESIS OF MOLECULARLY IMPRINTED POLYMER FOR DETERMINATION OF DILTIAZEM BY EXPERIMENTAL METHOD

Background & Aims: In this study, a magnetic molecular imprinted polymer was used to measure the diltiazem drug. Based on the structure and pharmaceutical agent group, methacrylic acid was selected as a monomer for Diltiazem. Ethylene glycol de-methacrylate and azobisisobutyronitrile were used as cross-linkers and polymerisation initiators, respectively. Also, chloroform was used as a porogenic...

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Fabrication of a Selective and Sensitive Electrochemical Sensor Modified with Magnetic Molecularly Imprinted Polymer for Amoxicillin

A modified electrochemical sensor for the determination of amoxicillin (AMX) was reported in this paper. The magnetic molecularly imprinted polymer (MMIP) were suspended in AMX solution and then collected on the surface of a magnetic carbon paste electrode (CPE) via a permanent magnet, situated within the carbon paste electrode and then the voltammetry signals were recorded. It was confirmed th...

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application of ion mobility spectrometry for determination of morphine in human urine

in this study, a rapid, simple and sensitive ion mobility spectrometry (ims) method with corona discharge as ionization source was described for the morphine determination in human urine. morphine was extracted and purified from urine samples using solid phase extraction procedure with c18 column. it can offer the clean extracts which no extra peaks were observed in ims. under operating experim...

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ژورنال

عنوان ژورنال: Analytical Sciences

سال: 2018

ISSN: 0910-6340,1348-2246

DOI: 10.2116/analsci.34.297